跳至主要内容

博文

目前显示的是标签为“Thermal Stability”的博文

A Chiral Three Dimensional Potassium(I)/Strontium(II)/Chromium(III) Oxalato-Bridged Coordination Polymer: Synthesis, Characterization and Thermal Analysis

Read full paper at: http://www.scirp.org/journal/PaperInformation.aspx?PaperID=52558#.VJtsjcCAM4 Author(s) Justin Nenwa 1 , Issoufou Kaboré 1 , Yves A. Mbiangué 2 , Patrick L. Djonwouo 1 , Peter T. Ndifon 1 Affiliation(s) 1 Department of Inorganic Chemistry, University of Yaounde 1, Yaounde, Cameroon . 2 Chemistry Department, Higher Teachers’ Training College, University of Maroua, Maroua, Cameroon . ABSTRACT A new compound of general formula {[(H 2 O) 2 K(μ-H 2 O)Sr] @ [Cr(C 2 O 4 ) 3 ]} n (1) has been synthesized in water and characterized by elemental and thermal analyses, EDX, IR and UV-Vis spectroscopies and by single crystal X-ray structure determination. Compound 1 crystallizes in the chiral space...

Preparation of MgAl LDHs Intercalated with Amines and Effect on Thermal Behavior for Poly(vinyl chloride)

Read full paper at: http://www.scirp.org/journal/PaperInformation.aspx?PaperID=52192#.VIj-cMnQrzE Author(s) Xiaoyu Xue * , Hongmei Zhang Affiliation(s) College of Chemistry and Chemical Engineering, Shanghai University of Engineering Science, Shanghai, China . ABSTRACT MgAl LDHs intercalated with CO(NH 2 ) 2 , NH 4 Cl and NH 3 ·H 2 O were prepared by co-precipitation and XRD, FT-IR, TGA-DTA and SEM techniques were employed for characterization. The results indicated that the layer-layer spacing of LDHs was enlarged by 0.169, 0.285 and 0.227 Å with the intercalation of CO(NH 2 ) 2 , NH + 4 and NH 3 , separately. The effects on thermal stability and degradation behavior of synthesized LDHs where mole ratios...

Effect of P Addition on the Thermal Stability of Nanocrystalline Ni-Co-Fe-P Coatings

Read full paper at: http://www.scirp.org/journal/PaperInformation.aspx?PaperID=51249#.VGAco2fHRK0 Author(s) Pinqiang Dai 1,2* , Lvbo Lin 1 Affiliation(s) 1 College of Materials Science and Engineering, Fuzhou University, Fuzhou, China . 2 College of Materials Science and Engineering, Fujian University of Technical, Fuzhou, China . ABSTRACT The thermal stability of nanocrystalline Ni-Co-Fe-P coatings with phosphorus content up to 3.38 wt% prepared by pulsed electrodepostion was studied using XRD, TEM and DSC. It is found that multi-component alloying does improve the thermal stability of nanocrystalline coatings due to a “solution drag effect”. For nanocrystalline Ni-40.41%Co-6.16%Fe-1.63%P coating, P-atoms ...

Synthesis and Characterization of Novel Sulphanilamide/Epoxy Resin Modified Polyester for Thermal Stability and Impact Strength

Read full paper at: http://www.scirp.org/journal/PaperInformation.aspx?PaperID=50697#.VEiV8lfHRK0 Author(s) Mohammed H. M. Alhousami 1* , Ahmed S. N. Al-Kamali 1 , Anjali A. Athawale 2 Affiliation(s) 1 Department of Industrial Chemistry, Faculty of Applied Science, University of Taiz, Taiz, Republic of Yemen . 2 Department of Chemistry, University of Pune, Pune, India . ABSTRACT The synthesis of thermally stable Tetra-di-glycidyl ether bisphenol-A (TDGEBA) Epoxy resin and Sulphanilamide (SAA) have been synthesized from (SAA) and TDGEBA by in situ polymerization technique to obtain Te-tra-di-glycidyl ether bisphenol-A Sulphanilamide (TDGEBA/SAA) Epoxy resin and modified with various per-centages of polyeste...