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Use of Ultrasound and Microwave Irradiation for Clean and Efficient Synthesis of 3,3’-(Arylmethylene)bis (2-hydroxynaphthalene-1,4-dione) Derivatives

Read full paper at: http://www.scirp.org/journal/PaperInformation.aspx?PaperID=50714#.VEmpfFfHRK0 Author(s)   Aldo S. de Oliveira , Luana C. Lianes , Ricardo J. Nunes , Rosendo A. Yunes , Inês M. C. Brighente Affiliation(s) Departamento de Química, Universidade Federal de Santa Catarina, Campus Universitário Trindade, Florianópolis, Brazil . ABSTRACT Nine 3,3’-(arylmethylene)bis(2-hydroxynaphthalene-1,4-dione) derivatives were synthesized through the reaction between 2-hydroxy-1,4-naphthalen-1,4-dione and different aromatic alde-hydes in water applying ultrasonic irradiation for 5 min at room temperature and microwave irradiation for 15 min at 70 ° ; C. Two of the nine derivatives, compounds 3-e and ...

Synthesis, Thermal Behaviour, XRD, and Luminescent Properties of Lighter Lanthanidethiodipropionate Hydrates Containing Aminogunidine as Neutral Ligand

Read full paper at: http://www.scirp.org/journal/PaperInformation.aspx?PaperID=48462#.VD4ViVfHRK0 Author(s)   S. Packiaraj , S. Govindarajan Affiliation(s) Department of Chemistry, Bharathiar University, Coimbatore, India . Department of Chemistry, Bharathiar University, Coimbatore, India . ABSTRACT Aminoguanidine lanthanide thiodipropionate hydrates of composition [Ln(Agun) 2 (tdp) 3 · n H 2 O ] , Agun = Aminoguanidine, tdp = thiodipropionic acid, where Ln = La, Pr, Nd and Sm if n = 2, have been prepared and characterized by physic-chemical techniques. KEYWORDS Aminoguanidine , 3 , 3-Thiodipropionic Acid , Rare Earth Metals , Spectral and Thermal Studies ...